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HomeMy WebLinkAboutCorrespondence SUB 4/18/2007 '.il 1;' : " ", ,," ~ ';., -~ ' "", SUB WATER DIVISION MEMORANDUM ;\. FROM: N.W. Corner 19th & Hayden Bridge, King Henry: Court Subdivision Chuck Davis: " " TO: DATE: April 18, 2007 ' " SUBJECT: Possible Meth Lab Contamination - updated ;,' , On 'April 17; 2007, Chu~k Da~i~ and Amy Chinitz (SUB) a~d 'Sha~n Krueger (City of'. Springfield) met on site with Mrs, Barnes to discuss the possible locations,ofwhere meth lab,' , wastes might have been spilled or dumped on the site, ':, :' . . ," , ' 'This meeting was a follow-up to Mr~, Barnes letter to the City:and the DEQ expressing her concern for contamination that may have occurre~ on the site that rimy have a public health impact to new property owners or to the public water 'supply, Chuck Gottfried (City of " " 'Springfield) asked us if SUB had dealt with similar situations and could we help develop a plan . ' for responding to Mrs, Barnes concern. '. ' . . - - ,We asked Mrs, Barnes to describe the site prior to it being leveled, so we could focus'our. , , investigation on areas most likely to have contamination residualS. We told' her that based on her ',' , description and recommendations, we would look for,areas where vegetation was stressed, soil' 'was discolored, and/or has an unusual odor to ,select locations for taking soil samples to send to ",' : the laboratory for analysis..',.,' .,.' .. ""I', ' , '.,' ,-' " ~ " ,-; ',. , ' ,. ... . .,' " . ,- ... . -" -~ , Mrs, Barnes said she believed the property had been a meth lab site, and that she had reported '. , that to the police on several occasions. She and her husband would watch activity from their' ',' ,home uSing a telescope. She pointed out an area in the front driveway where a niotor home was' " parked and suspicious activity took place, She also pointed out the foundation of what'ilsed to be ' a Quonset hut onthe northwest comer of the subdivision where she believed illicit activity' ' "occurred.' .,(.r .", .,.,'.' :""'"... ' ", ':;"';i:,; ,',',. ,,' ""...,' """";"':""~;_: ',\. . -. ';... . ~ . ,Mrs: Barnes walked the'site with us. Amy, Shawn:artdi c~niinued to~ajk the site after Mrs,; ". " , :, Barnes left, looking for signs of contamimition. The site had been disturbed as part of the, ' . ,,' . ,construction of the water, sanitary sewer, storm sewer, and other utilities. . The area where the , ,', " "", . ,driveway went to the previous residence was intact and we looked closely in the area where Mrs. ' Barnes said the motor home had been parked. We used a shovel to dig into the soil at eight (8), ',locations within a SO-foot circumference ofthe reported motor homes location. ,At each location'. " , where we dug holes, we 'looked for discoloration of the soils, and we each smelled samples of the . , soil.' ,In each case; the location was chosen because of its proximity to the driveway or because,. ,'. the vegetation was slightly yellowed. We did not find any areas adjacent to 'the driveway that; had any odor or soil discoloration. In each case, the soil had a.fresh odor arid there were night',' crawlers and worms that gave me an indication that the soil was not contaminated:' ' .'.. . . ':... -. -'. ," t'"" t,': ,;,. ,.' "".;':;.:"':<:'.::,l,, ' .' .". .t,:'. ,: ....,....,.:,:i':..;.". .' '1; " "..', '-. ....: .,,~_. . .:...,.,'....~". .....,'. i'. ,: .: " ;._"'.' . :""... ' <. '". "- ." ", ',~.~ \' ~_.', '.: . In the vicinity of the Quonset hut foundation, there was a deep'holewherea walnut tree stu~p was decaying thathadconcrete, pl,astic bottles, and other debri,sin-the hole, ,'fie dug several .,'::, ," .'. '" '. , " " .., ~ .'". '. ..,'. '.~ " ....r':. " ..;' '.,>.....:.;.. ..' ;:-. -, .\.' A '0";, <'.,: '." ,. ~.";'" .'; . .,'.. ~ ~-<,. , . " , .; l.:" ",,;"'-, ."."" "',"'." '- "o., ~ .', ", Memo to 19'" & Hayden BriL~ , King Henry Court . Possible Meth Lab . " ~"-" April 18, 2007 ", Page 2 of 2 .. holes adjacent to this looking for discoloration and odor. The soil did not have any unusual, odors or color. There were two locations on the outside of the foundation where we found discolored soil that did have an odor. In the northwest comer, there was an obvious location where motor oil had been dumped. In the northeast comer there appeared.to be motor oil and some other material that seemed more suspicious because of the odd odor.. " Shawn ,Krueger agreed to go to the laboratory ~nd pick up the,proper sample bottles for collecting a sample at the northeast comer of the Quonset hut. Shawn willcollect that sample on. ., Wednesday, April 18; 2007, and deliver it to Analytical Laboratories and Consulting in Eugene for analysis. We agreed that Springfield Utility Board would pay for the analysis and receive the results. ' ;.' Further follow-up will be determined based on'the results of the sampling. . . . Post script: Th~ draft of this memb was sent to Joe Leahy for his work with the City staff this .' afternoon (April 18, 2007). Joe asked that I have the results rushed. I 'called the lab at 4 PM and' . requested thatthe sample results be provided ASAP. I authorized rush turn around fees. The . results' will be available on Monday April 23, 2007 in the afternoon, They will fax the nisults. ., .. '., . ';l.., . , . " I~ " ''', '" , .' . .'~, ~ '. , .' .." ," '; /" " ';,\ ." ,~ .. :' ~ : ,',-, ,'i' ,',.. 'i:;'" _~ : 1 . i- " '.' -' , ~r -,.'. , ~ f' " " ',,"j :, ' ." . < . ' ..,' , ' '. .. " .' " ',' ," , ',I ;" ',.' '1,<. , . . I ~ . .:. , ~'...'. . ;. - -~..', .' '-'{ -:, -. ",- ',,' . '" . .~. ..:-:' . , ',.....(, ..... , ..'....,.','. --." .j' ~ .i, ,- -I ~:.,_. " , ",~ , . " ". ,,(I~,_- n.' .' , ',.,J' . . ,- -,. . ,. ~~. :::, '~.' ~ ," "I'.:,' " ~. 'Y . .' ',: " ,,'.:-.. ..i " ....." . , . , . ( / ~. ;',:....' ':.,' " I. ..... ': .... ",", ',- ~. '. " ", ." . . .. ~t ' . ,",' .' .'~ , , " " , , . ,,'~' ,., ~. ",. &: .p ,~ " . " . '; '.~ ':' i' "".': } ",',. ',:, 'f' 'I;,,'.':; " , :.. '. ,'1.'. ,,' '<,"t, ~ " , :.~;. ,J:. '. - ~ ,..';,:. . "~. 'J' , ,", ".J .-,.;, '. ,'. "'1 ' " ,. _.r . ,I ", ':." . , ,~ .' . ~ ,",_, " ." "<.;, ,:.~~. :'"'' -.~.. .. .~ ,;': 'f ~f-.. . ....~.". ,', c::~cu~~ts~~nd S'etti~~~umm?718\~Cal.seitings\TempOrary Internet Files\~LKAi\M.e;h Lab 19th' f1aYdenBridge~doc . '..':." . ' " ~ . , , . ..' ~ -.,', '.' . '!.'" ,j> .,. " " '". r {,- ',; ,';;' ..-:.' RPR-23-2007 03:19 P. 01/17 ~ 4 rIS Springfield U ljlity Board Water Division 202 S. 18th Street Springfield, OR 97477 p,hone: 1-541-744-3730 Fax: 1-541-747-7348 Fax To: Bret Sherry. Clandestine Drug Lab Program From: Chuck Davis, Water Quality Manager fa,,: 1-971-673-0457 Oat",: April 23: 2007 Phono: 1-971-673-0442 Direct line P"9"'S: 21 Re: Soil Samples ' cc: Joe Leahy, (541) 746-4109 Pie",," Reply .Comm"'nb: Bret As you can see trom the attached lab ,results there were no volatile chemicals detected, The met\lod used was 8260B that has method detection limits that range from 0.025 up to 1 mg/kg (1 PPM) . We appreciate the time you have spent with us on this issue, Would you mind calling Joe Leahy, Springfield City Attorney, and share the information you shared with me about the connections you have for working with property owners where thc possible clean up activities might be voluntary? He has questions that would be difficult for me to act as the intennediary and relay the information to everyone's satisfaction. Joe Leahy: Phone: (541) 746-9621 / S:\CHUCKDlWELLHEAD\2007-02'23 King Henel)' SubdMsion, soil sample,doc RPR-23-2007 15:39 p '" RPR~23~2007 03:19 P.02/17 [f=--------.----'.---.- .,:.---.~..~== ~ ::- ----~~-:...=';lC(:.,~.'::':',~:.~n.:_r:=rt!':"""::""'71:"":.:v,..,::~...:'= i Analytical Laboratory & Consult:mlts, Inc. ' 361 West Fifth A"enue. Eugene, OR 97401 541-485-8404 -1-800-262-5973 ,Fax: 541-484-5995 Orogo" ORELAP Accrodited ORELAPID OR100012 E?A 10 OR00016 ::;'7'"~_::r.~:;:I~:';:-: ~~ ':,~~:':;'.,,:, ;.';.:':;:. __ ,', 7:;~:"~:-;::';: ,"7; :", -';;:~';"'; ',;;' : i;' i\ Accn!dited in accordance with NELAC i Accredited a"alytes marked 'Y I (.="..- "._,...,.,.._.,.,.",,:,;i:[ I ~"~~~..:,:,:.".,':::.-,:;::. ~_........_.,.=:':':'.:::"_'::!=:=:-_':;'~."-' ':'OZ==.........__~.'::::.::".._.,.... -' '.. , t. This report presents the'results of the a"i;llyses of the sample(s) received on the date above and assigned the listed ALe !' lab report numbers. Test results relate only to the parameters tested and to Ine samples as received by the laboratory, ' Ii This report shall not. be reproduced, except in full, withlJut written consent of Analytical Laboratory & Consultanls, Inc, ""-", CASE NARRATIVE !: Ii " All analyses were performed according to the Analytical Li;lboratory & Consultants, Inc, Quality Assurance Program, All QAlQC requirements were met exoept as noted below, Analytical comments are noled with data flags on the reports and/or below, 1 'I " ',' I, I :! .1 :1 " ;: Volatile Organic Compounds by EPA,B260 B welt! analylell by Neilson Research Corporation. Medford OR. No anomalies associated witnlne analysis of the.se Sample(s) were reported, For results see ALe Report Page 5-8, ;i :! :; I' i: ;i :~ i' il il il i , ,i :1 " ;, I I L, "''=.__.~ "___._~__=::'';.;' '''~_______n =~~;.,__ _____. _ .__..!:;__'~~_~__....~ .. __. ,_"'___,~__ .______....,__ -----_..~_.'._.,.__. ~--- -. i_ . ~pproved /l~, jA "" -' /l ,,~___ ,I LabOratory Supervisor Date 4/23/07 .. = -., --_.,._--._-'-._..'~---_.,_._--_._~ -._._--_._."":.::.:::..::..-._._-:=.~.~~,,--';.'...._---,-"::-;...;...::.:::=- -.,~.-=-~:"'::~-:..":_~.:'==-=.:I 'I i " I: " II II I I :-:':":'::-.-""--;( 19957.95B.xls GENERAL RPR-23-2007 15:39 , Page 99% I of .;J 0 P.!'P RPR-23-2007 03:19 P.03/17 JNEILSO~!!JSEARCHI~~PORArIONU__ Enl'iro'nmental Testing Laboratory . , 04/23/07 Sandra Nordman Analytical Laboralory&Consultants Ine 361 W. Fifth Ave. Eugene, OR 97401 TEL: (800) 262-5973 FAX (541)484,5995 . RE: ALe 19957, 19958 Dear Sandra Nordman: Order No.: 0704447 Neilson Research Corporation received 2 s2rnpJe(s) on 04fi9/07 for the analyses presented in the following report. The results relate only to the parameters tested or to the sample as received by the laboratory, This report shall not be reproduced except b full, without the written approval of Neilson Rescarch Corporation. If you have any qll~:Stions .regarding theSl\ lest results, please feel free to call. ' , I, Sincerely, Neilson Research Corporation -l~k~ Fay LFowler Project Manager NRC - Page 1 or 17, ',ALe Report P"lI9 -3 ,of ;;i..O 245 South Grape Street 6 Medford.OR9'1S01_312J 6 (5411) 77()"5678 ~ fux (541)770-2901 RPR-23-2007 15:39 000/ D ~7 RPR-23-2007 03:19 P.04/17 r~:;;-' "'._H_'_=:=.~ ___,__ ----- --.---- -.-._.-._~-_._._~-_. ---..-. --...__._..~~-_.. .-.-..-.., ......~. , ---- --. --- - --- ------- ~-.._..,-""..~..". ....~ . "'-' ':'-"'""'.'-"". '". ".".. " "ij I' '; i i II Ir~A*~ti~;;.-r-ChUclkD;~i;;-==----'----'_._. '''~"~~';'rc'L''3-b R~p~rt"N~~'T,-19957=958-~c~=-cc""..,.,.==c,,=- ;":. II Client I Springfield Utility Board ._._.i' Dale Received L 4118107 OB47~~~~-=-~~'~! i-- .----"" --~~~i~~-f;::' ~if~~ 47;;".'.-" '- -- ..- =~~J. .6~:-:;::dn ~al::~i:::~~;;!.~~~;.~~;.~.~_ _,.,-----,-'-;; U,~~e:~o.___~~~~_~t:"'.,,""" ,-_..--,-...._--,.,,:,,_":;";"".,~_t ~~~;~~ Matrix___L.~~?~:ow" . ::,~_ ,~.~.=~=_~ ,:; VOLATILE ORGANIC COMPOUNDS EPA 826GB Analytical Laboratory & CtlnsultaJJlts, Inc. 361 West Fifth Avenue -Eugene, OR !17401 541-485-8404 - '1-800-262.5973 Fax: 541-484-5995 Oregon ORE LAP Accredited Laboratory 11;# OR100012, Accred;19d in accord""cll ..ith NELAC Acc",dllBd anulyte9 marked "~.. 'I Ii " ANALYSIS REPORT i' , I: j,i , \-~ I ,. I , '''~'._'''._'-----'~''-----::"...:..o..'':~''''J:.u:.:..=_'t:OI.'::'l:l:':';----" " " ".~~~~: ~,:;=:=",~~;~,:,,,,,::-,-;;:::::~~,".;::.~::~::,,~;:-:::,:':-::-,~::-.;:=-=:;.:~:::-=,::: :-:_-:::-.~:r.'.-;'=~ , , " :j I I, I' I I Analyzed by Neilson Hesearch Corporation, Medford, OR. Heport attached " ii Sample ID NRCID ClientJD 19957 19958 Oi'04447-01A Oi'04447-02A ;\ #1 #1 Dup '>:1. i " :i 'I i i , II I I I ! I il I: " ;' [; , i :, [ I; " 1 jl " I: I: i [' !.l !~ ;: " " h:=~=-- ...._.,._-~~~,~,'""-.,,~,,=_.- . -------,---___.. ~ _.__m.~~4~:.:.:.~..:..:...~:;"'~~=~'='_"':"i-...."':""'.;.,.~':.~=._ i ......--.-.,"-.. "'-" ,..I:::'~=~~~~'~~"':~=:-;-:-;=:;~~""",-.7": .:.~! 4123/07 i 19957 -9S8.xls Generic RPR-23-2007 lS:~q t'J~__ "'1 ')r-. RPR-23-2007 03;19 P,05/17 Neilson ReselJwch .Corporation 245 South Grape Street. Medford. Orogon 97501 541-770-5678 Fax 54'-770-2901 Analysis Repott (J~E.I.""'Il~"t~ EM OAlIOC~lI CLll'..N'I: Projett: , Lab Ord.r: Analytical LaborDtcry&Consultanlll Inc AJ.C 19957, 19958 0704447 Dale: Z3-Apr-07 CASE NARRATIVE The analyses were perfol'lTled aCGo~ding to the guide'lines in the Neilson Research Corporation Quality Assurance Program. This report contains anal)'iical results for the sample(s) as received by the laboj'atory. , Neilson Research'Cv'l'vo..tion certifies that this report is in compliance with the requirements of NEL1\P , No unusual difficulties were experienced during analysis of this batch except as noted below or qualified with data flags on lhcrcports. NRC - Pege 2 of 17 Page 1. of 1 . ALe Report PU9" lj of .;2 0 RPR-23-2007 l.S:41l OO~/ D "'" RPR-23-2007 .03:20 P.06/17 .' Analysis'R!'p,ort Neilson ReSetlrch Corporation 245 Soulh Grape Street. Medford, Or"Qon 97501 541-770-5678 Fax 541-770-2901 'Of:':EI..Q.~''1l1nn'5 I V~MtI"'(I:11 AD.h'llcKI L~bor.t.ry&Coo...II1lDlll Ioc. 36\ W. Fifth Ave, Eugene, OR 97401 Clien, Sample ID: ALe 19957 Sample Location: Springfield Project ALe 19957.19958 L.b Order; 0704441 NRC Sample ID 0704447-01A Colloction Date: 04118/078:30;00 AM Receivod Date: 04/19/079:1,0:00 Ml Reported Date, 04/231011:3l:38FM Matrix, Solid ANALYTICAL RESULTS NELAC Dilution : Ana\YI';' Aceredlted R...I, Qual MRL Unit/jl FlIctor DlItr: AflJloIY7.Cd .1 Vo/~ff1e Orger.ics by EPA 8260B Analyst: SA Y Acetone A NO 1 mQIKQ 04lZ3/07 Benzene A Nil 0,025 "'911(9 0412.3107 B.romobM2:9I'lB II Nil 0.025 "'9/Kg O4I2:J107 Bromochloromothene "- Nil 0,025 ",g/K9 04/23107 BromOdlcnlorom"l~nc . II NO ' 0,025 "'9/1(9 04123/07 BrDmore-rm A 1I11 'o.nzs "',rKg 041231n7 BrornomethMe A No 0" ",glKg 04123/07 2-ButB"C"C (MEK) A "0 mg/Kg 04/23/07 tert-Bulytbenzene A NO 0:025 "'91Kij 04/23/07 lIee-8lJl~lbentene I>- NO ~.~2S mgf)(g O~/Z3ro7 I't-BLltyltlen.tene I>- NO 0.025 mg'Ke 04123107 Carbon disulfide A NO o.OZS m~/K9 I 04/23101 Carbon tolr.u:I'UonOe A NO 0,025 mg/Kg 1 04/23/07 Cr.lorobs-n:tene A 110 0,025 mgfl(g 1 041'23/07 Chlcro~ane I>- 110 0.' mg/KQ , 04/23/07 Chlorororm A liD 0,0<5 mg/Kg , 04123/07 ChloromelhanD "- NO 0,025 mglKij 04'23/07 2-Cnlorotch,JE!ne A NO 0,025 mg/K9 04123107 4-Cl1lorOlolueno A- 110 O,OZS me/Kg 04/23107 , ,2'Dlbromo-J-c.hloroprop::lno A NO 0.5 mg/Kg , 04.123/07 OJbromochloromalhi5le A 110 0.0<5 m91K9 1 04/23/07 1,2-Dlbromo9tngne. (EDBI A 'NO 0,025 ",glK;g I 04/23107 DicratflOm&lh3!,o A NO 0.025 "'9/Kg 1 04t.'23r07 1.:?::Dlcl1lcrcb""~9ne A Ne 0.025 mg/Kg , 0C.J23f07 , .3.DlchlorObem:ene A Ne 0,025 mglKg , 04/23107 l,4-Dicl'llorobonzene A NO 0.025 mg/Kg , 04.123107 D;ChtoroC1inuC\ID~eth~nG {Freol\ 12} 'A NO 0,025 mO/KQ , 04123107 1. 1 ~Dlchloroethane ('. 1-DCA) A , NO 0,025 mQlKg 04123107 , ,:Z.D!chloro8(h3n~ (EDC) A NO 0.025 "Ig/Kg 04/23/07 1.1-Dichlol"Ct:lt'lone C1 ;1-0DE) A NO 0.025 mglKg 04/23107 c;s-',2.01d'iloroethylene A NO 0,025 mglKg 04123/07 tra~s:- 1 ,2-DJc.hIClrcathvlen~ A NO 0,025 mg/K:g 04123107 2.2~DlchIOrbpI'CJP:l"O A NO 0,025 mg/Kg 04',3(07 1 ,2~Olchtor:lpl'Op~lne 'A ,NO 0,025 m~IKg 0412310.7 QllQIIOll'rs: No - N'l:I( Delte'c-ct 31 the kcpon:iflg Umit S~ Spikt:.R~DVeT)' D\lI'SlCle :tc:c:cprcd rrcovery '~Itllt:s J - Al1elytc detecled below QuantitatiDn I"ml{$ R. RPD D\lISide-;u:ce-plt:d rcc:cvt'ry limits o . I\T\a\:1lt de-ICClcdiolhr: aU:Dti3~d Ml!thod Shmlc E. Value :lbove qu,a'llitoutln "'nsc .. - V~lul: C'Uc:ede M::.xlfl1um COnll1minBrJt ~C"\I'CI MRl ~ Minimum'iReport;nl1 limit NRC . Page 3 of 17 : Ale Repon Pall8 5 of ~o RPR-7,-;>~~7 'S:d~ ........~, n ~^ RPR-23-2007 03:20 .' P.07/17 Neilson Research Corporation 245 South Grape Slreet. Medford, Oregon 97501 541-770-5678 Fa~ 541-770-2901 A .. R H r' etl:'''~~tlUUIl'' nalYSfS eporfl . , ..,. O'M,,!' An.lyticol Labor9tory&Con,ul,nnfO Int 361 W. Fifth Ave, Eugell<, ,OR 97401 CU.", S:unpk!D: ALe 19957 S.mplc Locali",,: Springfield p.roject ALC 19957,19958 . ANALYTICAL RESULTS : Analyse!: l'JELAC A.~tredjted Result Qual 'MRL Va/aliI. OfT/.nlcs by EPA 82608 1.3.0Ichjo~propdl'le A 110 1,1-0iC:l1loropmpl!llnl!.i A NO or;-1.3-Dic:nloropropenB A- ND tr3n~.' ,3.0il:n.lofcpropcne A- ND .... Ethylbenrene A NO Hexachlcl'Obwadiene NO 2-H9Xanone A NO Isopropylben%One A NO 4-lscpropyltoluene A NO A-Ml:!:lh'l\~2.'P6m:a~onE A NO Motnyl [Oft-butyl eln8( A, NO Methylene> ChlorIde A NO Naphthallllno NO n-Propylbentene A No StyrBne A NO 1. 1. '.2-Tet~hlol'!)tHhane A 'lD l,l,2.2-TeuatnIOf'OOlhMe A NO Tetr:1C~IDfO(lt.nc"o (PCt:) A NO Toluene A NO 1,2:,3- Trjchlorobem:en~ A No 1,;;::,4... Trh;htcrnb@nzeM A NO 1.1,1-Tric.hIQroe1l1ane (1,1,1-TCA) A NO 1, '.2~Trlci\lDtDtllt'tQn~ ,. NO 7r1c"loroeln~n... (T'CE). A ND TrichloronuDrome(nane {Freon 11" A No '.2.3. TrlC!lloroprcpDn~ A ND 1,'2,4- TrilT'elhylbe-nUlM A NO , .J.5- Trlmnlhvlbeozone A NO VinVI chlorlae A NO Xyt9nSIl, Total A NO Surr; DlbramonlJoroll18lhaM 91.0 SUT'f: TalU8nlrdB 91.7 Sun: oIf-BrornonOOrobonzOr'lD 7~.6 0,0.. 0,0~5 0.025 0.025 0,025 0,25 , 0,025 0.0:15' O,D2fi 0.1 d.' 0.025 D.025 0,025 0.025 0.025 0.05 0,05 O.DS 0.025 0,025 0.025 D,025 0.5 D.025 O,D~S 0.025 oms o o o QlIllllfler.l'~ ND - Not Drftcttd At the. R.cpc:ln'nK Limit J - .....nal;ftl: detected below quant1t:uion Irmin B . A..n~lyt~ (ll:U:C:lla illlh! ~stx!i:lled MeUlt'a Blll'lk a . V~luc e::tc<<!ds Ml::timum Contaminam Le\lel S - Spike ((c~D"ery Cll.luldc ::rec:cpted rcccvt"ry limits R - R.P'O Oue\de nccepted ~t"O\lrry lim1U E. Value' above quamhatiol'l rat\gl: MRL - Minimum ;.R~ponins: Limi\ NRC - POlge 4 of 17 ~PR-?~-?~~7 1~:~~ L>b Order; 0704447 NRC Sample ID 0704447-01A Collection Dal'<; 04/18/078:30:00 Ai't Received D3Io: 04/19/079:10,00 AlII Repon.d Dale, 04/23/071:32;38I'M Matrix: Solid --~~ ._---,-.,. URilZ mglKg m9/Kg mg/tc;g mglKg mglKg !'T1gfKg mg/Kg my/Kg mg/Kg mglKg 1T19/K; mg/Kg mglKO mg/Kg m9,t(~ mglKg mg/KI1 mglKg mglKg mglKg rng:/Kg mglKg mg/Kg mgl~ m9lKg mglKg mg/Kg mg/Kg mgl!';g m;IK9 %REC o/"'EC '~REC ALe Report Pall. DilutioD Fac:tor Datt AnJllyz.cl1 , , 1 , Analyst: BA Y 04123/07 04123107 G4t23107 1H123/07 OM23/07 0<12310' 04f23/Di 04123107 04123107 O<lJ2310' 04123/07 04/23107 0412:3(07 041'23107 04123107 04'2.3107 0412310' 04123107 04/23107 04/23/07 04I23ro7 04123107 ,04/23/07 04/23107 04/23107 04/23107 0412.311>7 04/'23107 04123107 0'/~3107 04/23/07 0412'3107 04/23/07 ,'; 2 b of ;J..O APR-23-200? 03:20 P.BS/1? Neilson Rese,arch .Corporation 245 South Grape Street. Meclf()r(j, Oi'egon 97501 541-770-5676 Fox 541-770-2901 AnalysjstRePOrt I 01-'I:L4~1[1l1nJG 'i""'O,",n,,:1:' ADalytital L.bor.lllry&Consullants Ine 36) W, Fifth AVt. Eugent, OR 9740 I CliCJlt Sample!D: ALC 19958 Sample LOO.lion: Springlield Pro,iccl: ALC 1.9957, 19958 ANALYTICAL RESULTS , AnalYses, NELAC Accredited Result MRL Qual Volar/Ie Organics by EPA 82608 Acetone A NO Benzeno A NO 8t"C1mobenzene A NO aJl)rnC~lcromBltl8ne "- NO BromOCllchlcromelhs.I1e A i'lD Bromoform ,A NO Bromomott\ane ,A- ND 2~BulBnOl'le (MEK) A NO . tert.autylb8n:.:gn~ ,A NO ~ec-.Bu\ylbBn:tBne A /10 n-Butylbenzene A /10 Carbon di(l.\JlfitJe A /10 Carbon 1(!1r:Jt:hto~de A NO Ch1crobenzene A NO Chloroctilane A NO Chloroform A "0 Cl1lcrom~Hhan9 A NO 2-CI'lIorololuel1e A NO 4~ChJorOloluene A NO , .Z-OibromoA3-cI\lOropropDno A NO Dlbrcmochlofcrnethane A NO , .2-0ibttlmoethane (ED8) A NO O;bromOMe1hB!'16 A NO 1.2-DlchloroboA29ne A NO , .3-0id'lIoroberri(m~ A 1\10 1.4.oICI'IIOl'Dbon29M A NO DichlofOdlOuorcmeth3r1o (Frnon 12) A NO 1, '-Dlc;hlomefh3nEl r'. '~DCA) " "0 ',Z~OiC:hIDrDOlhalle (EDC) A "0 , .,.Dlchloroalh.n. (1. '-OCE) A NO CiB-1,.2-01cttlcraell\y1ene A 1'10 Irnng...1.2-0ichlcrtlothylenec A NO 2,2.DlchIDl'Ol'rOpana A NO 1.Z.01C::l1loriJ"roPS:M A NO , 0.OZ5 0,025 0,025 0,025 0,025 0, , 1 0.025 0.025 0.025 0.025 0,025 0.025 0,1 0.025 0,025 0,025 0,025 0.5 0.025 0.025 0.025 D,025 0.025 0.025 0.025 0.OZ5 O,OZS 0.025 0,025 0,025 0,025 0,025 Q~GunU'll: ND - NOI Dt1c:etttl allhe Rc:~tlrting Lim;t J . ATI.1lyte d'et<::clc:d below qU;lnlil.atilim limit!! B . ^"~1~ dlOtl:t"u:d itllhl: i1:;,~ol:i:lted Mt1hod Bliuilc . - Va-1m: cxc:ced!: MA.}.imum ConlAminant Le"'C'1 S - SpIke Recovery oUlrJdc: a~c:pled reeolJery limib R . RPO ouUidc acccplc:d roC:OV(1]' lim;t; E . V:lluC' ~bOVl:l q,u,,"limtion r.mgt PARI. - Mj~im\Jm Reporting Limit NRC - Page 5 of 17 APR-23-200? 15:40 Lab OtcleI: 0704441 JoJRC S:unplc ID 0704447-02.'1. Collection nate: 041181078:33:00 AM Received Dale: 041191079:10:00 AM RepDrted Date: 04!231011'3!,38 PM, Matti><: Solid Units mglKg mg/Kg mglKg m!#Kg mg/Kg mglKg mglKg mgfKg rog/Kg 109/Kg mgfKp rog/Kg mgl1<9 mglKg mg/l(g mg/Kg mg/)ol:;g mg/Kg mg/t(s mg/Kg mg/Kg mglK\l mg/Kg ITJg/l(~ mgll<g m911<g mglKg mg/Kg mg/Kp I'I1gl!<g. mg/Kg mg/Kg mgll<p mQ/1(s ALe ReDDrt Paa. 000/ Dilution Ffll~tor DJltt AJ1~}Y7.l'd , 1 1 1 An.lrs!: /lA V O4I2:l107 04(23107 04123/07 04123107 04123/07 04123107 04123/07 D-\fZJf07 04/23107 IJ41Z3fOT 04/2::3fD7 04,.3107 04123/07 04/2310i 04/23/07 D4J2:3{07 04/23107 04123/07 041Z3/07 04123/07 04113107 041ZJ107 04IlJI07 04/23107 04f2.!!f07 04/23107 04/2:3/07 Ollf23/07 04/23107 04123107 04/Zl107 04123107 04123/07 Q.arZ3/07 J 1 or ,;)0 D no RPR-23-2007 03:20 Neilson Research ,Corporation 245 South Grape Street Medford. Oregon 97501 541-770-5678 Fax 541-770'2901 Ana!ysis Repoiir; Analyiital Laboralory&CoDsultlUl!s lnr 361 W, Fifth Ave. Evgene, OR 9740 I Client S:unplo lD: ALe 19958 Semple LocoTio.: Springfidd Project: ALC 19957.19958 Or.r:l,;~llIlIIllr. - - 'IjPAOftClno,u Lab Order: 0704447 NRC Semple JD 0704447-0211. Collection. Da,<: 04/18/078:33:00 ",'\1 Received Dati:: 04/19/079:10:00 AM Reported Dare: 04/23/07 1 :3Z:38 PM Matrix: Solid ~~._-- ANALYfICAL RESULTS P.09/17 D 1] OU 1 \J ," 1 \J SJ SJ -J Neilson Research CorporatiDD CLIENT: W"ri< Order: Proj..l: Analytic,l uborotory&Consuhants Tnc 0704447 ALC 19957, 19918 Jl ,. D"e' lJ-Apr.07 D " ;u 'I I\J VJ 1 I\J ISl ISl -oJ --._-- -- ---~ ---..---- ---- -~ --- ANALYTICAL QC SUMMARY REPORT --. - - Run No: J.40S3 ISl VJ I\J ~ 5ampfe 10 MB-I2'912 SampType: MBlK Cliern 10: u.zzz. Bald1lD: 1291~ Amll~1e 1" ,... (') ::l:l ~ :> ;; .., .. ACetone Uenzoof! Bromob.enzen:e StomlXhloromeU,al1e Bromodicb'.oramelhane Bromoform Z Brom(Jmeth'ane . ;lJ 2,B.\aoon. (MEK) (') lert.Suly1benzene "R i:eo-Buty1benzsM ~ n-Butylbenune -...J Camoo disulfide So. Gatbon ~errach:oride ~ Ch.lorobeozene Ch~h8ne Chforofaml Ch!cr()metllarte 2-CNclIOtaluenlil 4-Ch!C1rotoluMe 1.2..0 Ibrtirno-3-ctlklropro pane OitlrC'mo<:ttIaromeu,ane- ..S) 1.2.0ibromoelhane (~DB) Dibrnrnamelhane ',:?Dkl'1~ooellll!r..e 1,3-Dich/.ofolMmzer.o 1.4...oi1::nfOlQbenzene Did1r(JTC<llltvcllJmelh~ne {Freon 12} 'J.I.mchlortJtl!rHlnS(1. '-DCA} 1,Z.OiclrloloolhEne IEOC) 2. J", o Re~ult " NO NO NO NO NO NO NO NO NO NO NO NO ND NO NO NO NO NO NO ND ND NO ND NO NO NO NO NO NO <)J3rjn<H~ ~~--~--- --'-- 1.0 0,025 0,025 0,025 0.025 0.1)25 0.10 1.0 O.lYl5 D.O:2S 0,025 0.025 0.025 0.025' 0.10 0,025 0.025 0_025' 0.025 0.50 0,025 0,025 0.G25 0,025 0,015 0,025 0.025 0.025 0.025 E 'I lluo::"l:.u'.<:'l1l.:ll,lil.!l;jijf1 "'flS':" ,~lp Hvl l:k:n:kd jllh~ ;\hf1im'Jm R'-l"lilih~ L;<llil --._-,-~----- -- --- ---_.~._- . ~---~- - --,- TC5tCode, EPA8260_S T~tCode: EPAB260_S Unfts: mgJKg l...lNo: EPA &28aS iEPA '5509) f->?ep (}af~: 04123.(07 _'1>16 Dale:, 04123107 Se-qNo: 51.21J9 MRL SFK \/Jlfue SPK ReI V'!l %REC UJy,limil "1~hLimil RPC ReIV~1 %RPO Rf'OUmil QuaJ II I!,,~,jfng f1rr,e..; (:h'l'rcpdnF:\If)'JI el'll}!i~ (c""'C<!~ R RPU ('!It.;:J= k''':>:f.'IL'<'1 f"'..,.CO'UTy hll'l.. J "'IoJI~I~ d-d~~ufl t1~kh~ YIjJr,tir..!J;I,n i':m;l-'; S S'~'"k.:: R''CfA'''')' ,1"lj.-:~le .1l;r:~.)tC.J r';>:,J\<:1')' hmil.' :u ~ ISl "- ~ -oJ Page I (J/J~) D U U I " ..J I " '" '" oJ Neilson Research Corporation .. ._._._'-~' ---- --- ------- -- CLIENT; Work On1er: l'raJect: Analytical Laboralory&Conru1t.ants we 0704447 ALe 19957, 19958 n ~ . DaCe: 23.Apr.07 D 1) ;t] I N 0J I N IS) IS) -J ~. --'..-' --.--- -----.- .. ---- -~_.- ANAL YTICAL QC SUMMARY REPORT T..,Cod.: EPAB260,,:S Samp:e 10 MB.'29"U Clief)(.IO: znzz. SeQN<l; 512U9 SampType: MOLK BaLch ro: 129'2 Anelll1e \, 1-O:Ohlon>elheM (l,l.OCE) , cls.1,2.Dich~oelh'l1l!llle lJa nll-1.Z-0icI110IoeUl)'ln ne 2,2.1)'ct1!atopropane 1.2"IJt(lhlotOpropane l,3-0fct'llortlpropane Z 1;1-lHchloroprtlpei'le ;IJ cis. L3-Dicf)roloprwene o lr.J1l-3-1.3-0lchl(lmprcpel'i'e Elt.)1t..am2rte H&X3Ch.!()(oootadier.o :> r- o :;u .. '8 ~ '" .2! .. ... '" .., <0 en 2-HexanClne a hoprupylbe:nzen& :::4 4--IS(lpropyll'ohlena .. 4.Methyl.2-()ei1b!l'1one Melh~1Ier1...oolyf elher _ M:th)~(\e dlk>ril1e ',1i1pf'tUulle.ne n- P rop)'1.be11zene Styrene 1.1,1,1- Tetra rhloroe{hatLe 1.1.2.~-TeuiiCt\roroelJ1ane Telnl cJ1loroelhen.e (Pee) lo~ue.ne. 1.2,3-Tricl1!.o-ltltrenze.ne 1.2,4- Tn'c.h1.orQobeITZene 1,1, 1.nk..htoro-elhane (1,1, 1.TCA) 1,1.2.Trtcliloroelh.3rlc Trichlc[OICUlenC fleE! o a 'G I) Result NO NO 1'10 NO NO ND NO ND NO NO 1'10 NO OlD NO NO NO NO NO NO NO OlD ND ND NO NO ND ND ND ND QolJlirio.: E '/.d':e.~lxIic:qUJ.1Il~t;"~r.:".t:." liD H.,-: O"'.,Xf....-.J ::.1 l!'''' l\Ii'li"ll.dTl R'(I':r1;r,~ Li.ii'lil TeslCode: EPAB~O_S Ulllls: matl<g TeW-':o: EPA82eOB IEPA 3550e. I.1Rl 0.075 0,075 0.025 oms 0,025 0,025 0.025 0.025 0,025 0.0.25 0.25 1.0 0.025 0,025- 1.0 0,025 0,10 0.10 0,025 0.025 0,025 0,025 0,025 0,050 0,050 0,000. 00<5 0,02.5 0.0'25 Prep Dale: ll4I2:'!I01 AndJy1i's Dale: f;Un:J101 AunNo: 34093 IS) 0J N ... SPK ~aJu.e SPK Ref Val %RE:C Lovrtimil HighUmil RPD Ref Val % RPD RPOllmil Qual H r.r.l.ii"n;i': limCl ipi" r.,\O{",nli;lr, \1' 1.n"I;,,~u- '~'::'>:l~'...I 1\ HPO ,...t.d!:d....!..CI.:.ql<unJ.;:\:lyl,:r1lit..~ ,\jl...lf)":G;(..-.;tJ;,lhd""'I.IU6nllwl;,J,-.bmiU :, Spi.:"", R.,-.;,:,ny (;"ui.!..: :li:'Xfl,:J roX,l' cry l~'n',ilj ... ... " ... -J 'U PflgC 20l10' D 1] 1] 1 \J .J 1 \J SJ SJ oJ NeilsoJi ReiieilfCO Corporation -- -.- -----.._._~ - C1.ll!NT; Work Order~ Projec-(: Amlytic.J ulx"alory&Co,,-,uJlan" Ine 0704447 ALe 19957, 1995B - - - --- -~---- ---'--- - -- ---.,-- ~- .~- .-----.-.------...- -.-----..--. -- ---_._--~_..- - -----------.-- '---- --- ------ DOle: 2J-Arrr,07 ANALYTICAL QC SllMMARY REPORT ~ ~ Sample 10 M8-1'2S12 CL~Jj' to: ZZ2Zz T~ICode: EPA8..26'O_S UlIl'LII: mq/Kg T.'INo: EPA 8260B IEPA 35-508) Prop Oata: 00If73J07 AI1iIr,.sfs Dale.; 04/23107 RunNo: 34M3 SeqNo: 5111 39 SampT~jl'e: MBLK 9ah:h to; 1.2912 AniJt)te Re.iulf MRL SPK value SPK R,' Val TrtchJoro~OIO-mei:hane(Freon 'J} 1,2,3'Trld1{~ropr~ne 1.2.4-Trimeth~1'~l'\UIne 1,3;S.r rlmeitly1lJenzene Vinyl cI1l0rid. m,p-X)fene Z Q-X)1ene ~ X~ie11eS. Total n Suo: O<.",,"unuorom'lh>o. Sun: TallJ'lHle-da SUIT; 4-Brnmofhltyobenzelle NO NO NO NO NO NO ND NO 1.035 a.BS50 0,025, 0,00 0.025 0.D25 0,025 0,050 0,025 0,075 o o V "U '" ., OJ \D ' a Sampk? 10 ~ ellen/CD:' I 1 1 . r\ d...... ......... , "IV o o o Te3ICod.: EPAR160_S IIAEC Lol'<Fmil H;ghLlmll APO ReI Val %RPD RF'OUmil ai/a.1 104 89,5 ' 81.4 70 70 70 100 ~:lO UnIt,,: m~Kg lePA35~081 LCS-11912 UZZZ SampT;'P.: LOS Balch 10: 12912 T~(Code: EPA62G(LS. TeslNo: EPA !~lJ9 !: ~' o I f' " , ). }~ AnaI\1. Re..slltt MRl. SPK vawe SPK R:eP/al' Ace!ane 2.100 1.0 2.5. 0 ~nlene 1,064 0-02S 1 O. 8!omobf!nzene 1.026 0,025 I 0 Blomochlornmetf1~e. 1.052 '0,025 I 0 81tlmQdldtkJromelhane' 1.038 0-025 1 0 Srnmoform 0,9180 0,075 1 0 7,Bu..""". iMEK) 2,55" 1.0 2,5 0 lert.Butyfb-cnzen-e 1.052 0-025 , 0 SE'c-gl:f)1~I1lEln-e 1.0!1-.4 0.025 I 0 n.{julylbenlCIle 1.1'31 0,025 1 0 C:Jf'tion letradl.'on'dl!' UOl' 0-'125 1 0 Chlon:Jboemene 1.000 0.0'25 1 0 Chlorofonn 1.192 0,025 0 ---- ---- J ) Qadlir,tn: E V~lu.:: ::.i;;(l~<: qtdr.llr.lIic" r.JI,g<: N() ,'(':1 l>..:r:-:.:I.-d;:J the .\\;niml.'m :("fh"l;ll~ llli1il " !-r,:,'rFnJ: 1m:....'): ror ~'/l;V.l fiHio;l r:r a':-Jr:i')'S -~_ICl; iUc,j ~(_rD ,,:.w.i,J~ ~c~p:':d r.:.:.,,:.'.,1")' lim;l; ..\r.ilf)1,;,U(,1...:u.lbc!rI.'...I1":.....rild,I'H1I,.lli:.,; )" Sl-"ik..: I{.;:....-c~ ;;::y uJC;; d.,. ~ L:t<:i'r..:J r~""J\ t'T)' ~;' IT. ,0; ,':'0 Plep [}alc: 04I2J107 RtmNo: :J4IHlJ I AnalY$is'Da!e: 1W23107 SeqNo; 51.2.140 "REc t.owUmn HlghUmil RPO Ref Va'l %RPO RPDUmil Qval 84,7 65 1~5 100 65 1'35" 103 65 135 105 65 135 104 55 135 Q7,8 65 135 102 55 ' 1:15 1[).5 65 1305 109 65 1:J.5 113 65 135 110 65 135 10' 65 135 119 65 135 -----'--~-- Page.1 fJI If) D '1l ;U 1 I\J ,(,.j 1 I\J IS) IS) -oJ IS) (,.j I\J ~ ''1l ,,' 0::........ ol\J " ~ , " -oJ " .' ~ D 'U ;U I OJ ,(,.l I OJ 1SJ 1SJ '" J1 '" .j. r- n :D 01' '0 J 0 ;0. ! ... ~ - /-' g, 10 0 J" Neilson Research Corporation ._------_.~------ ---- ---- - ---'--.--.-- - --. -- -- -_._-~-_.-. -- ------------.- ..- --- CLIENT: Work Order: Proje<l: ADalytieal Labot1llor)'&CoJ\SlJIl3nt> lne 0704447 ALe ]99~7. 19958 Sample 10 lCs,.1'2:912 CEoollO; u.uz SampTypt'; lCS B,'ci1IO, llg12 Anal\1e 2-Ch.Ion:llCJkJene 4..ch!QfOlo]uenc 1.2-0ibromo.~hlo~pruparu!l Oibf('lfllocl1~romettJane ~ .2-0ibramo.elhallo8 (EDB) Olbcvmcmel11en.a Z 1.2-Dlm!c]tllberrze~ ;;0 1,3--0ic.hrGtoflenzene (') 1.....0icblcf'IJlM!n:zene iJ t, i.Ol~hlfJreei~nS! (i .i-OC....j ~ 1,2.0kllloroeth;ene tEDG) 0; t.1~Dich6oroelhene (I ,1-OCE) g ds-1,2.0JchkJrceU1)iene ...... tJGns-I.Z-Oil::hlc(Oelhylene -...I 2.2-Oichlorl1pl<Jp!J1e 1,2~Dkhroroprop;ilM 1.3-DlchloruproPilne;, 1,1.uiehkllTiprot}EM'" os-1,3-Dichloropl"Opefle b1I n,..... f, 3-0icl'1fowpcopenc EIl1)'flJ<l12ene Hex.ad'lror~.dBdiene 2;He.xanol1.e IsopropylbeozeflC ....1.sopropyUolueoe <t:UAll1ryI-2-penfaoone "'t&thyllert-tJutyl t:U'"l€t Ml'-Uly1Me d1!oride N.!!!~hUlafEr;e Resull 1.150 1.161. '.2J4 1.020 ",02 l.11G 1.10.\ '-068 t.OM i. loa 1,150 0.9170 1,076 0,9195 1.11l-' 1.114 1.105 1.152" 1.0\4 1.0BB 1.116 1.174 2.0JO 1.054 1.074 2,24:l 1.134 0,0015 1.043 Qll.!.'Win: G 'hJut "t-,lV: ('.""nnl~lic"," /3";;~ NO tto:l u..;~t~J II 10< fltlll;fTI,im fh-p<lllin;.: !.Imll TutCOOe: EPA.&Z60...::S Unil~: mgI1<g 7..',,"0: EPAB2BOB IEPA3MOBj MRl 0.025 0.025 0.50 0,025 0,0Z5 0.025 0.025 0.G25 0.025 v_G~5 oms 0.025 0,025 0.025 oms 0,025 0.025 '0,025 0.0'25 0.025 0.Q25 0.25 1.0 0.025 0,025 .1.0 0.025 0.10 0.10 0 115 65 0 116 65 0 123 65 0' 102 65 0 110 65 0 112 65 0 110 65 0 109 65 0 106 65 G .. . 55 ,.. 0 115 65 0 91.7 65 0, 108 6,<; 0 96,0 65 0 120 65 0 'II 65 0 110 65 0 115 B5 0 101 65 0 109 E-5 0 112 65 0 117 65 0 61.2 65 0 105 65 0 101 65 0 69,7 65 0 113 65 0 99,2 65 0 10' 65 --- SPJ< valoe SPK R@fYal 1 1 1 I 1 1 I I I I 2.5 I I 2,5 1 1 1 Dale: 2J-Apr,07 D " ;u I OJ L-J I OJ 1SJ ISl '" ----- ---- -- ------~-- ANAL YTICAL QC SUMMARY REPORT T."ICode: EP1\.8160_S Prep Date: 04123101 Analysis Oate: 0.tJ2'JJ'07 AUllNo: J.40i-J Se.qNo: 5121-tO 1SJ L-J OJ >-'" %REC lu-.,,1..tmit Hlghlimit APD Re'VaJ 135 135 135 135 135 135 135 135 135 %RPO RPOUmil Qua~ ~3S 135 135 135 135 135 135 135 1:15 135 135 135 IJ5 135 135 135 1:15 1:J.5 135 135 ,\r Jhl~ U-::-;~;;:l.:d o.:l".'i '~'I::.nllL11i"tl illl';!..; ~ ~'~II~~.~ k......'l..~ry (\1I,-,j.1~ .l.:.c:::f';-;J t'::l.:'IHrt li'Tliu II 1{,~'('I;.1i t'n'..;) 1'10" FIt"I;ilr;;~.on oll(.J.1)1i;s t.~~.;C(r,xl R KI'[J ,H;lli~c :J';:O::;l(~J rt;(;Il":crj I:n,;ti '1] >-'" L-J "- >-'" '" F'agr .f uf Iv D 'lJ ;U , OJ (,,1 I OJ \SJ \SJ -J Neilson Research Corporation ---------- --- ------- -. -- -- -- ----- "----.--- CLlENT: WDrk Order: Proj'<:(: An.lytical laboraJoI)'&Consultan':'!nc 0704447 . ALC 199.17, 19~.I8 ~ Vl " OJ Sample '0 LCS'f2!l12 SampTtpe: les Tes.feode: EPA82eo -$ Unit;,: mglXg Clienll0: = BsIct1ID: 1~g.12 Tes.tND: EPA !t2~lJB (ePA 355081 ......1)1. Rasull MRL SFK \"<1lue SPK Rei Vat n-Prol"l1be<u.!ne 1.f54 0.02'5 1 0 S~""ne I,D3f 0,025 1 0 l,1.1,Z.TeUal;hlo,o6tt1ane 1.072 o.02~ I 0 1; J,2.2.Tetr;c:hrcroethane 1.036 0.025 1 0 TelTaChlo'''''Ihene (peE) 1.024 0,025 I 0 Torl.'elle 1.052 0,050 I 0 Z J,2,a.rrichlorobemene 1.112 0.050 1 0 Al 1,2.4-T ,ithfQt'ob<en1 ern! 1.132 (lOSO 1 0 (1 ,,1. t.Tricl1t.araelhale (1.1.1.rCAj L21e o.ois 1 0 1] 1.1,2-rrichJlHCetm:ne 1.077 0,025 I D III <0 Tric.h~Ul~ (TeE) 1.116 0.OZ5 I 0 .J> ~ 1.2,J. Trkhforoprapane 1.026 0.50 I 0 ::..J. 2- 1,2.4- TrimelhY;b.enz~ne 1.152 0,025 1 0 ~ 1.a,5-Tn-meth)1treruene 1.110 0,025 I 0 "" m.p.X~tenQ ',31. 0,050 2 0 (J.Xytel1e 1.06<1 0.025 , 0 x'tren~. Tolal 3.362 0.075 3 0 SUIT:' DlbromolJuaroll1etfHille 1.000 0 1 0 SUrr. TahIernH18 'O.97~O 0 1 0 . Sun: 4.8ron\olfUfJrubenzene 0.93S0 0 1 0 5.3mple lO 0104441-D1AMS S.mpTYJlo: 1.1$ Te:;ICcJIl/lJ: EPAB'260_S Unils: mgiXg Clif:nt 10: AJ.:C 19957 Barch [0: U912 T""'No: ePA 6260B tEPA 3950B) > r (") '" .. " o 'l 0" o! ".. Ana1)" Resull MRL SPJ< ya!ue SPK Ref Val 1.661 1,0 2,5 0 0.6%.5 0.025 , 0 0.8715 0,025 1 0 0.6.920 0.025 I 0 .~-_. w Acelone EJEntEne BrumClhellz(ne- Br<HTlocl:iOHllTlE:tt..a ne !l. I !J o CJL'allfi.r.I: E V":"'::Jti,,'': l:j'J:u:til~lill.l r.!:"S~ ~;-o ~,',,( Prl:lo::t:l""lllh~ ,V,in;ruLIT: !{q:':'.n;fl~ li..-ctl " " II'JI:lI<'"g, l;,T,,;j. kr r;'(I:'~nl:!m f,r 1,'1)':,.)1.i ~~r"':~ed RI'[) '""ui;1'.:-:.~HJ:~~~J rec.;,'", ry lin1l1,) ~ " "- ~ -J o , V.'e: 2J'Apr,07 D 'lJ ;u I OJ W " OJ \SJ \SJ -J --- -- --'---"-"- ---_. --.~- ANALYTICAL QCSUMMARY REPORT T..1Code: EPA8260_S Pll!p Date: Colf2JI07 RunNo: 34 1)93 Arralysis Dare. a~f2.J.!01 S<>qllo: 512140 %REC. lo'h'limil HIgt.Lfmil Af'O Ref Vat %RPO RPOl'm" Qu., 115 .5 13~ 103 65 135 1117 65 135 10;4 65 135 IOZ 66 135 105 65 J::rS '1' 65 135 113 65 135 In 65 135 108 6.5 ~J.5 1'2 65 135 10J 65 135 fl5 65 135 116 65 135 II. 65 135 107 55 '35 113 55 135 '_IOij. 65 135 97.6 .5 135 03.9 65 135 \SJ W I\J OJ Prep Data: 04'J23J07 Ana~s" [}a,.: 04l2Jto7 AunNo: 14093 Seq/okJ: 512 143 %REC LowUmiJ Highlimil RPO Rof Val %RPO RPOLirnil QI1a.I 65.4 89,S B7,Z 89.2 55 65 65 65 135 135 135 135 ..---------------- - - ----~.~ --- 'lJ .~ H..11)1~ cld'" Int he~;w Cl;'~rll~ii.:w ii""IL.; .' ;{ri~c. R~("'H(,,.. ;;~l";i,',,,: IC.:q::.-;\ t((l;~~:l' li:Tl>ts {.u~t! 5 olIO D 'U ^' 1 I\J (,,1 1 I\J IS) IS) '" Neilson Research Corporation ----- .~--------_..----- ---- ---- ------ CLIENT: Work Order: /'toJect: Acalyticsllaboralory&CONlJlla.n\3 JlIC 071M447 Ale 19951. 19958 Jl " I\J U,'e: '1J-Apr.1J7 D 'U ^' 1 I\J LJ 1 I\J IS) IS) '" --. -- .---.--.--"- -~.- ------ ---- ANALYTICAL QC SUMMARY REPORT o o. o o o o o o o T..,!Code: !,;PAR260_S Prep Da!&: 1W2-3101 Runf.l'o: :I(()9~ A(\2Ilysi.sDate: O4I2J/01 SoqNo: 512T43 ~RE.C lo\\u-mu HighUmil RPD Re.f Val %RPD APOUml1 altai 86.7 65 Iy,; 00,8 65 135 76,2 65 135 00.2 55 135 00,7 65 135 02,7 65 135 93.4 65 135 03.~ 65 135 102 65 t:l5 ;;.~ ;s t"'''' ~ 90.0 85 135 95.6 65 135 65.1 65 135_ 60,2 85 135 91.4 65 136 92.0 l>5 135 92A 65 135 9L8 65 135' 95,4 65 135 96.8 65 135 7&.0 65 135 93,0 55 135 86,8 65 135 102 "5 135 94,0 65 135 91.0 65 135 95,8 65 135 83,8 65 135 BB.J 65 135 IS) LJ I\J I\J SaropType: MS Ba1cl110: 12912 TeslCode: EPAmlSO..;...S Units: mg/Kg r..lNo: EP4 B2~OB IEP4 J~B) .5alllp!a 10 OT04441.o1AMS Crlent ro: ALe; 19957 Arta~'fEll Re!lull MRL Bromcdicl1lQfomeUlafte 0,6065 0.025 BromoCorm O.wao 0,025 2'Butar"l1fl (MEKJ 1,856 1,0 , lert-ll1J~1b"w,". O,OOZ5 0,02-5 5ec-Bu.Mben~n9 O,SOIO 0,025 n~Buty1!.:elllene 0,9270 0.025 Z Catbonfehath~~e 0,9335 0,025 lJ Cf1klrobenzene 0.9330 0.025 ('l Chloroform 1.019 0.D25 ~ Z..c1i:..u@lij:iiCii.c O.3~2~ :.1,025 ., (0 4-Cl1~oror(]ll1ene O,09S0 0,025 .. ~ 1.2.0ibrnmo..Jc.chIoropropane 0.9555 0.50 tv 0 D.OlomDd1toromelhane 0.B510 0.025 ~ I,Z.Olbrome<th... (EDB) 0,8915 ~ 0,075 ..... OLt.romumelhane 0;9135 0.01.' 1,2-Oic.ltrOtube<neI18 0.0200 0,025 r,3-Dlc/l'orobenZl:!na 0,9235 0.0'1.5 .1 ~4-0lcMoml:;l(! ru ene 0,9115 . 0.025 )> I,'.DicNo,,,,,lhan'IJ;1,DCAI 0,9545 0.025 .- .1.2.Dh::~lataEUlane (COC) ('l 0,9<;80 0.025 ;0 I.I.o;chloroelh.". (1, ',DCE! 0,1195 0,025 " '" l::.~ 1,2- Did1'oroelJ',y1em~ 0,9375 0,025 0 .:l- t121ls-I.2-0IohloroE.t.hY:ene 0.6690 0.1]25 't7 ! 2,2.OfcJlloropmpane 1,018 0'(;'25 .. I, '2-OiciJrOlO'pfopane o 0385 O,()25 1,J...Dicl1roroplOpalte ' 0,910' 0,02. -'- I, HY.chloroplopelie 0.9580 O,C'~5 cis. ~.3-D1cNorOiltop.ene O,8,)~5 0,025 S. mos.' .J...Dir.NOfUfl'op.<!ne 0.B1>-30 0.025 ,> ----- --- Uu,tln~rl: ,. \',IJe a!Nv(;t!'.untiUlllllI r':"I.!:'.( J 0' ND ,'; ,,\ 0.: 1\;10; I c..~ ill 11...: .\1;.1 i, II' t;n 11 ;:;:... III f1 ii 1..1 r, I ( , SPK vatulO'! I I 2.5 I 1 1 1 1 1 1 '1 1 1 "1 " 1 1 1 ,1 '1 1 1 1 1 1 I I SPKRe/V$.I o o o o o Q o '0 o o o o o o o o o o o (; ~r,~I}'~c Ik:~I.-,;) Ix'.)w ll,U3.i11IUliolllirnllj: S Si'i~<: Rn'-'.lfy'....IU~[t..: ]".x<:pre.j "-.,:,,.nyt;:niu 'U " 11."-!.1lr,g lim<:; r~Jr P"~I'Jr:Jl:iJfl i;r ,F1i1::r3i~ ""l~r::r.kJ K 1',t'IJ..-JL",;"J,: .J,....."'ll(~,1 f\X(l\-,ryliillll\ 'r". I'age" af IV ~ V1 " ~ '" D 'U ;0 , \J CJ , \J SJ SJ -oJ Neilson Rcs~arch Corporation. --- .--------- -~---~ CLIENT, Work Ord." Proje"'C~ Analytical Lo.bDlaID<)'&CoD'ollllnl> Ute 0704447 ALe 199.'17, 19958 ~--- --.. _. --. --.-- - ---_._---------_._----~ -- - Dale: 2J-Apr-07 D 'U ;0 , I\J <.., , I\J IS) IS) --J ANALYTICAL QC SUMMARY REPORT Testeode: EPA8260_S Jl ". \J SampType: M5 Barch 10: 11912 Sampfe ID Or~7001.AMS Clierrl to: ALe 199"57 Al1<3Iy1e " Res\lU- F: C1 :0 . ~ J'" JU 'I . Ethy,l~ l1.lene Haxllclf<<obuLullen..e 2......,f!JIJ;m0l1e 1~t:-(af1}llf-enzene . .tl.l.!;a IJ fop)1loluene 4-M''Cl:hyl-2-pe..ntaftOne Z ^te.tf\~1 lerl...t.utyl eUler .::tI c",tel11yl'elle (Moride o Naplllharene. ;:; n.Propytbenzene ~ Styrene ..... l.l.1.2~TetrachkHoe:Ulane '" 9.. t.1,2.2-TelrachtorolltJullle Tetrilchloruethene (peE) ~ Tolueo8 1,2.3- Tricnrortlbef'1re"ne 1, '2.4- TrichlorClblffizece ,,','.TIichloroell1....lI.,,'.TCAJ 1.1,2.Ttict1orocl1Hlle. fric hlmoeUn ne (Tee) T.'l.~Tn-d1.lOrojJrOfl.anc 1.2.4- TrimeU1)ibemet1E1 1.J.5- Trimel")it>eme.ne m.p-Xyren(! Q.-':';yfeoe Xylefles. To-tal Sun: DibromoR'llDfomettJanr:! Sun: T~ruenl'!:-d6 Sl.lrr. .s.S/omOnllorobl:oDzEne O,!lSl~ 0,6415 1.661 0.9015 ,0.8950 1.758 0.95J0 0,8250 0.8320 0,98.0 O.alSO' 0.9110 0,8015 0.8050 0,8915 0,8555 0.8890 Ul41 0,8870 0.9'25D 0,8320 O.99I~ 1.012 1,972 0,9110 2.883 0,8940 0.8020 0.7755 L,--' a. '/J o Qallnlr'1: E Vli'J~_ ,1.-:,,;,: 'l.:JJnl;l..Jli~" r.i11i." ffU N.ll O>::''L:,.,J ~ I~,,~ .\!i";RU11 :,~ :.t1i.1J l;'nil . TeslCode: EPAIJ260_S Vnils-: m;JKg re,lNo, EPA82eOB (EPA J~8) Prep Dale: Wnto1 Analy-sis_Da4e: 04J21tOT. IS) c.J I\J I\J MRL SPK....IlU! SPK Re'Val '!SREe 0.025 I 0 %.2 0.25 1 0 84.2 1.0 2,5 0 66.7 0.025 1 0 90,2 0.02~ I 0 89,5 1.0 2.' 0 /0.7 0.025 I 0 .95.3 0.10 I 0 82.5 0,10 1 0 83.2 0.025 1 0 98,6 0.Q25 1 0 07,5 0,025 1 0 91,1 0,025 1 0 66,8 0,025 I 0' 86.3 0,050 I 0 89,2 0.050 1 0 85,6 O.{]50 1 0 6a.9 ~ 0.025 1 0 104. ~, '0,025 1 0 88.7 0,025 1 0 92.5 0,5IJ I 0 83.2 0.Q25 1 0 99.2 0.025 I 0 101 0,060 2 0 98,6 0.025 I 0 91.1 0.0/5 J 0 ~6,1 0 1 0 ""A 0 1 0 80,2 0 1 0 17,6 RunNo: 3-4'D9J SeqNo: SIl143 Low1..,im.ll ~igMjmll RPO ReI Val If Il<J:.lni':, i\fT.,:,:; fl'f [lri:f"'lr~(io 1 '111,UlYloi. ~~;(-;-,j,.1 /l Rrn .1'Jlid~' ::""~/H<:,j r<:,~,'~'~I)' li,r.il-; %RPD RPDUmil OU<tJ 65 05 ~ 05 65 65 65 65 65 65 65 65 65 85 65 65 65 00 65 65 65 65 85 65 55 85 65 65 65 1:15 155 135 1:15 .55 1:15 135 1M 135, 135 135 135 135 135 135 135 1J5 135 135 135 135 135 1M 1M 135 , 135 135 135 155 '\11;.11,,[.: t!o:-t.::.:k:1l]du..... C.U.l<1I,t.;lil1n I;",ih :::; 'ij:-il..-e Rl:C'(I~-.::rYII:.JI,!.Jo:= !.(~\-'I,;..,1 ~~~n\-~""",li-m;11 'U Iluge lof 10 ~ 1]), "- ~ --J }. \ D ~' 'U ;u Neilson Researcb I Corporation DaCe: 2J-Apr-1J7 D N W ------ ----~--_. ------- .------- .----.-....: ----..----. ---_._.~-- 'U I "- ..----;;---.- .-_. - .----.---. - - .--- -.------ - .~---- ;U N Cl..IIlNT: Analyticdl LaboIatory&Coruullanls lnc I \SJ ANAL YTlCAL QC SUMMARY REPORT N \SJ Work Order: W -J 07044 47 , N PIojecr~ ALe 19957, 19958 TcslCodc; EP AS2 60 S \SJ ~ i - \SJ Vl , -J " Sample ID. 010<<41.o1.IMSD SampType: M50 lutCode: EPAB280_S Unil.$.: mgIKg F'n~p Dale: O4J':;IJJOl RunNo.: 3409.l \SJ N C!JenIID: Ale '5557 T..,No: EPA 8260B Se"qNo: 513146 W S,'eh 10: 11511 IEPA 3&.5 OS) Analysis Oafe: o.tn3ro7 N N Ana:~1e Result MRL SPK va:U9 SPK Ref Vel %REC lo'Ntimit H1BJlUmil RPO ReIV," %RPD RPOl!mil Q",' Al;lelone 2.006 1.0 25 0 80" 65 135 1.661 16,9 25 Benzene 0.8005 0.0'<5 I 0 86.8 65 ';15 0,6955 1.12 25 Bt1lmcbenufle 0,6680 0.026 I 0 llQ,e 65 135 0,8715 0,402 2,5 BromochJornmelhane 0,8000 0.025 1 0 80,3 65 135 0,892 0.112 25 "Orcmodlc.hlofomeU1ane 0,!l555 0.Q25 " 0 85.6 65 '1J!j 0,8665 \,26 25 B..'Om(lrnrm 0.&005 0.025 I 0 60.0 65 135 0,809 0.933 25 Z 2.Butanone (MEK) 1.9<6 1.0 2.5 0 n.o 65 135 '1.5I!ifl 0,3114- 25 ;U lert,SlItylbenzef1e 0.6080 0.025 1 0 69,8 65, 135 0,0025 a.5UO 25 0 tl!'trBlIrylbenzen'3 65 135 0,901 0,769 25 0.9140 O.OZ5 1 0 g1.~ " i1.Ctt:-l~~'::~<:;.1c C.SSOO nn.,.,. < 0 9-5.0 !!5 f:!5, (1.927 2'.45 25 OJ v....u;.... , "" (A,rbQn Isbln;hloride 0.6925 0.025 U 69,2 65 135 0.0:}35 ~.49 25 '" ~ ChlDrllbenzene 0,0125 0,025 0 91.2 65 135 D.9"J3 2,22 25 ... Ctltarorarm 1,019 25 9- 0,9910 0.025 0 99.1 65 135 2,79 ~ 2.chklrofDlue{le Ol!ll45 0,0'25 0 96.4 65 135 0.9925 Q,601l 25 --.,J 4-Cl1lcm!ohrene 0,0000 oms 0 99.0 55 135 0.99$1 0.905 25 , .2-0iblom0-3-chloroprap3ne 0.OS10 O.ti() 1 0 96.1 65 155 Om;55 2,6:] 25 DitllOmoc:hI(llom~ne O.&3W 0.025 1 0 63,2 65 1;15 0.051 226 25 . 1,Z.(Jitlromoefn-<JlTaIEDB) O,661!O 0.026 l' 0" 68'9 65 135 0.8915 0,281' 25 ~ DI~rom(lme!hane 0.9205 0.025 1 0 92,0 65 135 Q,9135 0.763 ,25 :-J 1,2.DichlcHlXICf\l.ene 0,5!H; 25 II 0.9260 0.025 1 0 92,6 65 135 0,9205 . 1.3-Oichrorc.ooruene 0,9145 0.D25 1 iJ 91.4 65 1:15 0,9235 0,0'19 25 D i 1.4--0ichlorlJ-b.cnlene 0.9195 0.025 1 92,0 1:1-5 0.9175 0,218 25 D a 65 " " '.1.0id1lon;.l:lha~e (1, l-DCA) O.~436 / ! 0,015 1 0 114.5 1\5 1:l5 0,95<5 1,00 26 . 1.2.Did1JOI'oel11..ne IEOC) 0,9490 0.025 I 0 94.9 65 J:15 0.008 1.98 25 1.J.QichkH-oettlene (1, '.DeE) 0.7690 Q,025 1 0 16.9 65 135 0.n95 1,21 25 Q ciS'.1.?-Dic.hloroeln)U!l1e . 0,9250 0.025 , 0 92.5 65 135 0,9J75 1.34 25 - [nn:i-1.2.DtGhlomelh)1'eoe O,e520 0.D25 1 0 65.2 85 135 0,009 1.98 25 a. 1,2.0icMoroplopane 0.0045 0.025 I 0 96.4 .5 135 '.016 5,35 25 1.2.-Oichl,uopftlj:J,;,ne 0.93-50 0.Q25 I 0 9J.5 65 135 0.9395 0.480 25 --< l> 0 -~--~ ---- ---.--- .---- --< 0 C.)U..'ifj"li: C V~l''': 2b:.'.~ q'!~"l;i:,lit.n n.'lg<: " I In Uln,'t l:J.1.C, (.,i P"-<=~QJ'Jlil)r1 (f ~...:ll'.,,: ~ .-: ';;<:'.'fJJJ (\I.~" I..: ,10;'...;:;1.&..1 t.:l,-.",' 'l~ FliL;I:._~n li",i~, 'U D or ~il, Not 1><I...:t~l'.;! ItlO: I-lif;~'-I,'-'", 1-\\;j.lJI~;IlI: Li01"" " !1l'llr"JL!,;!c ~(..-o:;;:!..;;r (_:"-:U',.,."/ 1;",,;1, , ~;~:i~ , :{.~ .l"~! 'I "" L, i,t.) -~.:..:.tfi~ ,f r ("l<}~': I)' l.:rr.:li ~ . 'U l;o.ge.'iofIO -J ~ " ~ ~ -J -J